Tuesday, May 20, 2008 - 3:50 PM
Medical Arts Building, Rm M-134 (Queensborough Community College)
473

Kinetic and Equilibrium Studies of Small Molecule Binding to (PCP)RhI Pincer Complexes

Mark D. Doherty1, David C. Grills1, Kuo-Wei Huang2, Dmitry Polyansky1, and Etsuko Fujita1. (1) Brookhaven National Laboratory, Upton, NY, (2) National University of Singapore, Singapore, Singapore

The binding of small molecules such as N2, H2, C2H4, etc., to coordinatively unsaturated transition metal centers is an important first step in their activation and conversion to useful chemicals.� Thermodynamic and kinetic parameters governing this process in (PCP)RhI pincer complexes have been examined using a variety of techniques including UV-vis flash photolysis, time resolved infrared (TRIR) spectroscopy and NMR spectroscopy.� Results will be discussed in the context of a proposed mechanism for small molecule coordination to transition metal complexes.

The research carried out at Brookhaven National Laboratory was supported under contract DE-AC02-98CH10886 with the U.S. Department of Energy.